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SPX1-b: Certified Calibration Solution for 13-desmethylspirolide C

From National Research Council Canada

Alternative titleSPX1-b : Solution d'étalonnage certifiée pour la 13-déméthylspirolide C
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DOIResolve DOI: https://doi.org/10.4224/crm.2018.spx1-b.20180119
AuthorSearch for: 1; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council of Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; SPX1-b; 13-desmethylspirolide C; spirolides
Abstract
CRM-SPX1-b is a certified calibration solution for the determination of spirolides by chemical analysis methods. Each ampoule contains ~0.5 mL of a solution of 13-desmethylspirolide C in methanol with 0.05% trifluoroacetic acid at a concentration of approximately 7 µmol/L.
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
13-desmethylspirolide Cmass fraction6.360.30µg/gcertified
13-desmethylspirolide Cmass concentration (15-30 °C)5.010.24µg/mLcertified
13-desmethylspirolide Cconcentration (15-30 °C)7.250.35µmol/Lcertified
Publication date
PublisherNational Research Council of Canada
Copyright statement
  • © 2018 National Research Council of Canada
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References
View items (12)
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  5. Cembella, A. D., N. I. Lewis, and M. A. Quilliam. ‘The Marine Dinoflagellate Alexandrium Ostenfeldii (Dinophyceae) as the Causative Organism of Spirolide Shellfish Toxins’. Phycologia 39, no. 1 (January 2000): 67–74. .
  6. Investigations into the toxicology and pharmacology of spirolides, a novel group of shellfish toxins (1 January 2001). .
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  8. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  9. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
  10. Pauwels, Jean, Andrée Lamberty, and Heinz Schimmel. ‘The Determination of the Uncertainty of Reference Materials Certified by Laboratory Intercomparison’. Accreditation and Quality Assurance 3, no. 5 (4 May 1998): 180–84. .
  11. Ellison, S. L. R., S. Burke, R. F. Walker, K. Heydorn, M. Månsson, J. Pauwels, W. Wegscheider, and B. te Nijenhuis. ‘Uncertainty for Reference Materials Certified by Interlaboratory Study: Recommendations of an International Study Group’. Accreditation and Quality Assurance 6, no. 6 (18 May 2001): 274–77. .
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CollectionCanadian Reference Materials and Methods
Record identifier130c439a-5265-403f-83a4-c49bc096ca30
Record created2020-09-09
Record modified2025-04-22
Date modified: