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PTX2-b: Certified Calibration Solution for Pectenotoxin-2

From National Research Council Canada

Alternative titlePTX2-b : Solution d’étalonnage certifiée pour la pecténotoxine-2
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DOIResolve DOI: https://doi.org/10.4224/crm.2013.ptx2-b.20120516
AuthorSearch for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: 1
Affiliation
  1. National Research Council Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; pectenotoxin-2; CRM-PTX2-b
Abstract
CRM-PTX2-b is a certified calibration solution designed for analytical method development and accurate quantitation of PTX2. The concentration of CRM-PTX2-b makes it suitable for preparing a dilution series for calibration of liquid chromatography (LC) and liquid chromatography-mass spectrometry (LC-MS) instrumentation, as well as for spiking shellfish control samples for recovery experiments.
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
pectenotoxin-2mass fraction5.580.16µg/gcertified
pectenotoxin-2mass concentration (20 °C)4.400.13µg/mLcertified
pectenotoxin-2concentration (20 °C)5.130.15µmol/Lcertified
Publication date
PublisherNational Research Council Canada
Copyright statement
  • © 2013 National Research Council Canada
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References
View items (6)
  1. Yasumoto, T., M. Murata, Y. Oshima, M. Sano, G.K. Matsumoto, and J. Clardy. ‘Diarrhetic Shellfish Toxins’. Tetrahedron 41, no. 6 (January 1985): 1019–25. .
  2. MacKenzie, Lincoln, Patrick Holland, Paul McNabb, Veronica Beuzenberg, Andy Selwood, and Toshiyuki Suzuki. ‘Complex Toxin Profiles in Phytoplankton and Greenshell Mussels (Perna Canaliculus), Revealed by LC–MS/MS Analysis’. Toxicon 40, no. 9 (September 2002): 1321–30. .
  3. Toxicology and diversity of marine toxins. Gupta, R.C. (Ed.) Veterinary Toxicology: Basic and Clinical Principles, 2nd edition (15 March 2012). .
  4. Regulation (EC) No 853/2004 of the European parliament and of the council of 29 April 2004 laying down specific hygiene rules for food of animal origin (30 April 2004). .
  5. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  6. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
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CollectionCanadian Reference Materials and Methods
Record identifier5c885c4c-8612-4611-a7b1-ee33317a161f
Record created2022-04-05
Record modified2025-11-20
Date modified: