AZA2-c: Certified Calibration Solution for Azaspiracid-2

From National Research Council Canada

Alternative titleAZA2-c : Solution d’étalonnage certifiée pour l’azaspiracide-2
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DOIResolve DOI: https://doi.org/10.4224/crm.2022.aza2-c.20220623
AuthorSearch for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Name affiliation
  1. National Research Council Canada
Format3D, Material
SubjectCanadian reference material; azaspiracids; azaspiracid-2
Abstract
CRM-AZA2-c is a certified calibration solution for analytical method development and accurate quantitation of AZA2. The concentration is suitable for preparing a dilution series for calibration of instruments such as liquid chromatography with detection by mass spectrometry (LC–MS), as well as for spiking control samples for recovery experiments.
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PublisherNational Research Council of Canada
Copyright statement
  • © 2022 National Research Council of Canada
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References
View items (5)
  1. Tillmann, Urban, Malte Elbrächter, Bernd Krock, Uwe John, and Allan Cembella. ‘Azadinium SpinosumGen. et Sp. Nov. (Dinophyceae) Identified as a Primary Producer of Azaspiracid Toxins’. European Journal of Phycology 44, no. 1 (February 2009): 63–79. .
  2. Satake, Masayuki, Katsuya Ofuji, Hideo Naoki, Kevin J. James, Ambrose Furey, Terry McMahon, Joe Silke, and Takeshi Yasumoto. ‘Azaspiracid, a New Marine Toxin Having Unique Spiro Ring Assemblies, Isolated from Irish Mussels, Mytilus Edulis’. Journal of the American Chemical Society 120, no. 38 (1 September 1998): 9967–68. .
  3. Kenton, Nathaniel T., Daniel Adu‐Ampratwum, Antony A. Okumu, Pearse McCarron, Jane Kilcoyne, Frode Rise, Alistair L. Wilkins, Christopher O. Miles, and Craig J. Forsyth. ‘Stereochemical Definition of the Natural Product (6 R ,10 R ,13 R , 14 R ,16 R ,17 R ,19 S ,20 S ,21 R ,24 S ,25 S ,28 S ,30 S ,32 R ,33 R ,34 R ,36 S ,37 S ,39 R )‐Azaspiracid‐3 by Total Synthesis and Comparative Analyses’. Angewandte Chemie International Edition 57, no. 3 (15 January 2018): 810–13. .
  4. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  5. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
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CollectionCanadian Reference Materials and Methods
Record identifier5cdf5f6c-0cec-4df5-bee6-03a4fead2cd0
Record created2022-12-20
Record modified2022-12-22
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