| Alternative title | HIPB-1 : Matériau de référence certifié de plomb de pureté élevée pour la fraction massique du plomb, masse atomique, la composition isotopique et les impuretés élémentaires |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2020.hipb-1 |
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| Author | Search for: Meija, Juris1ORCID identifier: https://orcid.org/0000-0002-3349-5535; Search for: Methven, Brad1; Search for: Tong, Shuoyun2; Search for: Mihai, Ovidiu1; Search for: Swider, Katarzyna1; Search for: Grinberg, Patricia1ORCID identifier: https://orcid.org/0000-0002-1167-6474; Search for: Mester, Zoltan1ORCID identifier: https://orcid.org/0000-0002-2377-2615; Search for: Yang, Lu1ORCID identifier: https://orcid.org/0000-0002-6896-8603 |
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| Affiliation | - National Research Council Canada
- State Key Laboratory of Geological Processes and Mineral Resources, China University of Geosciences, Wuhan, PR China
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| Format | 3D, Material |
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| Material type | High-purity material |
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| Subject | Canadian reference material; HIPB-1; lead; isotopes of lead; atomic weight |
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| Abstract | HIPB-1 is a high purity lead Certified Reference Material (CRM). A unit of HIPB-1 consists of approx. 1 g of high purity lead wire. This material is intended as a primary standard for the determination of mass fraction of lead and as an isotopic standard of lead. |
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| Analytes | View analytes| Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| lead | mass fraction | 0.999990 | 0.000002 | kg/kg | certified | | lead | atomic weight | 207.1791 | 0.0002 | 1 | certified | | lead-204 | isotopic abundance | 0.012822 | 0.000012 | mol/mol | certified | | lead-206 | isotopic abundance | 0.27096 | 0.00008 | mol/mol | certified | | lead-207 | isotopic abundance | 0.203511 | 0.000026 | mol/mol | certified | | lead-208 | isotopic abundance | 0.51271 | 0.00010 | mol/mol | certified | | 206Pb/204Pb | isotope ratio | 21.133 | 0.014 | mol/mol | certified | | 207Pb/204Pb | isotope ratio | 15.873 | 0.014 | mol/mol | certified | | 208Pb/204Pb | isotope ratio | 39.99 | 0.04 | mol/mol | certified | | 204Pb/206Pb | isotope ratio | 0.047319 | 0.000030 | mol/mol | certified | | 207Pb/206Pb | isotope ratio | 0.75107 | 0.00022 | mol/mol | certified | | 208Pb/206Pb | isotope ratio | 1.8922 | 0.0010 | mol/mol | certified | | 204Pb/207Pb | isotope ratio | 0.06300 | 0.00006 | mol/mol | certified | | 206Pb/207Pb | isotope ratio | 1.3314 | 0.0004 | mol/mol | certified | | 208Pb/207Pb | isotope ratio | 2.5193 | 0.0008 | mol/mol | certified | | 204Pb/208Pb | isotope ratio | 0.025010 | 0.000026 | mol/mol | certified | | 206Pb/208Pb | isotope ratio | 0.52849 | 0.00028 | mol/mol | certified | | 207Pb/208Pb | isotope ratio | 0.39694 | 0.00012 | mol/mol | certified | | lithium | mass fraction | <0.06 | 0.07 | µg/kg | certified | | beryllium | mass fraction | <0.04 | 0.02 | µg/kg | certified | | boron | mass fraction | <0.1 | 0.2 | µg/kg | certified | | carbon | mass fraction | 25 | 300 | µg/kg | certified | | nitrogen | mass fraction | 3 | 30 | µg/kg | certified | | oxygen | mass fraction | 53 | 500 | µg/kg | certified | | fluorine | mass fraction | <0.6 | 1.5 | µg/kg | certified | | sodium | mass fraction | 12 | 100 | µg/kg | certified | | magnesium | mass fraction | <0.1 | 1.5 | µg/kg | certified | | aluminium | mass fraction | 1 | 25 | µg/kg | certified | | silicon | mass fraction | 0.4 | 2.1 | µg/kg | certified | | phosphorus | mass fraction | <0.09 | 0.24 | µg/kg | certified | | sulfur | mass fraction | 5 | 5 | µg/kg | certified | | chlorine | mass fraction | 33 | 170 | µg/kg | certified | | potassium | mass fraction | <6 | 7 | µg/kg | certified | | calcium | mass fraction | <2 | 25 | µg/kg | certified | | scandium | mass fraction | <0.05 | 0.04 | µg/kg | certified | | titanium | mass fraction | <0.05 | 0.41 | µg/kg | certified | | vanadium | mass fraction | <0.04 | 0.16 | µg/kg | certified | | chromium | mass fraction | <0.07 | 0.04 | µg/kg | certified | | manganese | mass fraction | <0.07 | 0.04 | µg/kg | certified | | iron | mass fraction | 0.4 | 1 | µg/kg | certified | | cobalt | mass fraction | <0.05 | 0.03 | µg/kg | certified | | nickel | mass fraction | 32 | 6 | µg/kg | certified | | copper | mass fraction | 170 | 90 | µg/kg | certified | | zinc | mass fraction | 7 | 4 | µg/kg | certified | | gallium | mass fraction | <0.3 | 0.2 | µg/kg | certified | | germanium | mass fraction | <0.6 | 0.6 | µg/kg | certified | | arsenic | mass fraction | 0.5 | 0.3 | µg/kg | certified | | selenium | mass fraction | <2 | 1 | µg/kg | certified | | bromine | mass fraction | <0.8 | 2 | µg/kg | certified | | rubidium | mass fraction | <0.1 | 0.1 | µg/kg | certified | | strontium | mass fraction | <0.04 | 0.03 | µg/kg | certified | | yttrium | mass fraction | <0.04 | 0.06 | µg/kg | certified | | zirconium | mass fraction | <0.06 | 0.03 | µg/kg | certified | | niobium | mass fraction | <0.03 | 0.02 | µg/kg | certified | | molybdenum | mass fraction | <0.3 | 0.2 | µg/kg | certified | | ruthenium | mass fraction | <0.5 | 0.7 | µg/kg | certified | | rhodium | mass fraction | <32 | 50 | µg/kg | certified | | palladium | mass fraction | 12 | 5 | µg/kg | certified | | silver | mass fraction | 5330 | 1600 | µg/kg | certified | | cadmium | mass fraction | 2070 | 600 | µg/kg | certified | | indium | mass fraction | 0.7 | 1.5 | µg/kg | certified | | tin | mass fraction | 6 | 3 | µg/kg | certified | | antimony | mass fraction | 0.5 | 0.4 | µg/kg | certified | | tellurium | mass fraction | <0.3 | 0.2 | µg/kg | certified | | iodine | mass fraction | <0.07 | 0.18 | µg/kg | certified | | caesium | mass fraction | <0.09 | 0.13 | µg/kg | certified | | barium | mass fraction | <0.1 | 0.1 | µg/kg | certified | | lanthanum | mass fraction | <0.03 | 0.02 | µg/kg | certified | | cerium | mass fraction | <0.02 | 0.01 | µg/kg | certified | | praseodymium | mass fraction | <0.1 | 0.3 | µg/kg | certified | | neodymium | mass fraction | <0.08 | 0.4 | µg/kg | certified | | samarium | mass fraction | <0.6 | 1.5 | µg/kg | certified | | europium | mass fraction | <0.3 | 0.8 | µg/kg | certified | | gadolinium | mass fraction | <0.5 | 1.3 | µg/kg | certified | | terbium | mass fraction | <0.1 | 0.3 | µg/kg | certified | | dysprosium | mass fraction | <9 | 23 | µg/kg | certified | | holmium | mass fraction | <0.1 | 0.3 | µg/kg | certified | | erbium | mass fraction | <0.4 | 1 | µg/kg | certified | | thulium | mass fraction | <0.1 | 0.3 | µg/kg | certified | | ytterbium | mass fraction | <0.4 | 1 | µg/kg | certified | | lutetium | mass fraction | <0.1 | 0.3 | µg/kg | certified | | hafnium | mass fraction | <0.1 | 0.1 | µg/kg | certified | | tantalum | mass fraction | <240 | 400 | µg/kg | certified | | tungsten | mass fraction | <0.2 | 0.1 | µg/kg | certified | | rhenium | mass fraction | <0.2 | 0.3 | µg/kg | certified | | osmium | mass fraction | <0.7 | 1 | µg/kg | certified | | iridium | mass fraction | 1 | 3 | µg/kg | certified | | platinum | mass fraction | 13 | 4 | µg/kg | certified | | gold | mass fraction | <32 | 30 | µg/kg | certified | | mercury | mass fraction | <14 | 11 | µg/kg | certified | | thallium | mass fraction | 580 | 120 | µg/kg | certified | | bismuth | mass fraction | 1200 | 360 | µg/kg | certified | | thorium | mass fraction | <0.06 | 4 | µg/kg | certified | | uranium | mass fraction | <0.06 | 0.09 | µg/kg | certified |
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| Publication date | 2020-04-01 |
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| Publisher | National Research Council Canada |
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| Copyright statement | - © 2020
National Research Council Canada
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| Access condition | |
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| References | View items (9)- Guide to the expression of uncertainty in measurement (GUM) (1 January 1993). http://www.iso.org/iso/catalogue_detail.htm?csnumber=45315.
- Meija, Juris, and Zoltán Mester. ‘Uncertainty Propagation of Atomic Weight Measurement Results’. Metrologia 45, no. 1 (8 January 2008): 53–62. https://doi.org/10.1088/0026-1394/45/1/008.
- Meija, Juris, Brad Methven, and Ralph E Sturgeon. ‘Uncertainty of Relative Sensitivity Factors in Glow Discharge Mass Spectrometry’. Metrologia 54, no. 5 (15 September 2017): 796–804. https://doi.org/10.1088/1681-7575/aa83d6.
- Wang, Meng, G. Audi, F. G. Kondev, W.J. Huang, S. Naimi, and Xing Xu. ‘The AME2016 Atomic Mass Evaluation (II). Tables, Graphs and References’. Chinese Physics C 41, no. 3 (March 2017): 030003. https://doi.org/10.1088/1674-1137/41/3/030003.
- Tong, Shuoyun, Juris Meija, Lian Zhou, Brad Methven, Zoltán Mester, and Lu Yang. ‘High-Precision Measurements of the Isotopic Composition of Common Lead Using MC-ICPMS: Comparison of Calibration Strategies Based on Full Gravimetric Isotope Mixture and Regression Models’. Analytical Chemistry 91, no. 6 (7 March 2019): 4164–71. https://doi.org/10.1021/acs.analchem.9b00020.
- Yang, Lu, Shuoyun Tong, Lian Zhou, Zhaochu Hu, Zoltán Mester, and Juris Meija. ‘A Critical Review on Isotopic Fractionation Correction Methods for Accurate Isotope Amount Ratio Measurements by MC-ICP-MS’. Journal of Analytical Atomic Spectrometry 33, no. 11 (2018): 1849–61. https://doi.org/10.1039/c8ja00210j.
- Sturgeon, R E, B Methven, S N Willie, and P Grinberg. ‘Assignment of Purity to Primary Metal Calibrants Using Pin-Cell VG 9000 Glow Discharge Mass Spectrometry: A Primary Method with Direct Traceability to the SI International System of Units?’ Metrologia 51, no. 5 (25 June 2014): 410–22. https://doi.org/10.1088/0026-1394/51/5/410.
- Dunstan, L.P., J.W. Gramlich, I.L. Barnes, and W.C. Purdy. ‘Absolute Isotopic Abundance and the Atomic Weight of a Reference Sample of Thallium’. Journal of Research of the National Bureau of Standards 85, no. 1 (January 1980): 1. https://doi.org/10.6028/jres.085.001.
- NIST SRM 997: Isotopic Standard for Thallium (23 July 1986). https://www-s.nist.gov/srmors/certificates/997.pdf.
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| Referenced by | View items (10)- He, Juan, Juris Meija, Xiandeng Hou, Chengbin Zheng, Zoltán Mester, and Lu Yang. ‘Determination of the Isotopic Composition of Lutetium Using MC-ICPMS’. Analytical and Bioanalytical Chemistry 412, no. 24 (16 December 2019): 6257–63. https://doi.org/10.1007/s00216-019-02271-6.
- Huang, Zili, Chaoqun Wang, Rui Liu, Yingying Su, and Yi Lv. ‘Self-Validated Homogeneous Immunoassay by Single Nanoparticle in-Depth Scrutinization’. Analytical Chemistry 92, no. 3 (8 January 2020): 2876–81. https://doi.org/10.1021/acs.analchem.9b05596.
- Xu, Shifen, Linghong Zhan, Chengyi Hong, Xiaomei Chen, Xi Chen, and Munetaka Oyama. ‘Metal–Organic Framework-5 as a Novel Phosphorescent Probe for the Highly Selective and Sensitive Detection of Pb(II) in Mussels’. Sensors and Actuators B: Chemical 308 (April 2020): 127733. https://doi.org/10.1016/j.snb.2020.127733.
- Li, Ziyan, Hongmei Li, Dongyan Deng, Rui Liu, and Yi Lv. ‘Mass Spectrometric Assay of Alpha-Fetoprotein Isoforms for Accurate Serological Evaluation’. Analytical Chemistry 92, no. 7 (7 February 2020): 4807–13. https://doi.org/10.1021/acs.analchem.9b03995.
- He, Juan, Lu Yang, Xiandeng Hou, Zoltan Mester, and Juris Meija. ‘Determination of the Isotopic Composition of Gadolinium Using Multicollector Inductively Coupled Plasma Mass Spectrometry’. Analytical Chemistry 92, no. 8 (8 April 2020): 6103–10. https://doi.org/10.1021/acs.analchem.0c00531.
- Flierl, Lukas, Axel Pramann, Janine Noordmann, Anita Röthke, and Olaf Rienitz. ‘UncorK – A Monte Carlo Simulation Tool for Calculating Combined Uncertainties Associated with Mass Bias Calibration Factors for Isotope Ratio Measurements’. Spectrochimica Acta Part B: Atomic Spectroscopy 168 (June 2020): 105866. https://doi.org/10.1016/j.sab.2020.105866.
- Lin, Ran, Jie Lin, Keqing Zong, Kang Chen, Shuoyun Tong, Lanping Feng, Wen Zhang, et al. ‘Determination of the Isotopic Composition of an Enriched Hafnium Spike by MC‐ICP‐MS Using a Regression Model’. Geostandards and Geoanalytical Research 44, no. 4 (29 July 2020): 753–62. https://doi.org/10.1111/ggr.12343.
- Kanan, Sofian M., and Ahmed Malkawi. ‘Recent Advances in Nanocomposite Luminescent Metal-Organic Framework Sensors for Detecting Metal Ions’. Comments on Inorganic Chemistry 41, no. 1 (4 September 2020): 1–66. https://doi.org/10.1080/02603594.2020.1805319.
- Zhu, Xiang-Kun, Jacqueline Benefield, Tyler B. Coplen, Zhaofu Gao, and Norman E. Holden. ‘Variation of Lead Isotopic Composition and Atomic Weight in Terrestrial Materials (IUPAC Technical Report)’. Pure and Applied Chemistry 93, no. 1 (1 October 2020): 155–66. https://doi.org/10.1515/pac-2018-0916.
- Karasiński, Jakub, Andriy Tupys, Lu Yang, Zoltan Mester, Ludwik Halicz, and Ewa Bulska. ‘Novel Approach for the Accurate Determination of Se Isotope Ratio by Multicollector ICP-MS’. Analytical Chemistry 92, no. 24 (23 November 2020): 16097–104. https://doi.org/10.1021/acs.analchem.0c03768.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 6547228a-b07c-4d9a-8a70-9d1b9acb5f7e |
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| Record created | 2020-12-12 |
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| Record modified | 2025-11-20 |
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