| Alternative title | ASP-Sca: Matériau de référence certifié de tissu de pétoncle pour l’acide domoïque |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2026.asp-sca.20221123 |
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| Author | Search for: Perez Calderon, Ruth A1; Search for: Reeves, Kelley L1; Search for: Baribeau, Danielle1; Search for: McCarron, Pearse1ORCID identifier: https://orcid.org/0000-0002-7746-8432 |
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| Affiliation | - National Research Council Canada
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| Format | 3D, Material |
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| Material type | Matrix material |
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| Subject | Canadian reference material; CRM-ASP-Sca; domoic acid; scallop tissue; amnesic shellfish poisoning |
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| Abstract | CRM-ASP-Sca is a scallop tissue matrix certified reference material (CRM) designed to test the accuracy of entire analytical methods for the quantitation of DA. This may include, but is not limited to, sample extraction procedures, separation methods, and evaluating instrumental techniques including liquid chromatography with detection by ultraviolet absorbance (LC–UV) or mass spectrometry (LC–MS). |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| domoic acid and C5'-epi-domoic acid | mass fraction | 10.7 | 0.8 | µg/g | certified | | domoic acid | mass fraction | 10.5 | | µg/g | information | | C5'-epi-domoic acid | mass fraction | 0.2 | | µg/g | information | | isodomoic acid E | mass fraction | 0.7 | | µg/g | information | | isodomoic acid D | mass fraction | 0.6 | | µg/g | information | | isodomoic acid A | mass fraction | 0.1 | | µg/g | information | | isodomoic acid F | mass fraction | 0.05 | | µg/g | information |
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| Period of validity | - Valid from 2026-01-09
- 1 year from date of sale
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| Storage conditions | |
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| Publication date | 2026-01-09 |
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| Publisher | National Research Council Canada |
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| Copyright statement | - © 2026 National Research Council Canada
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| References | View items (6)- Wright, J. L. C., R. K. Boyd, A. S. W. de Freitas, M. Falk, R. A. Foxall, W. D. Jamieson, M. V. Laycock, et al. ‘Identification of Domoic Acid, a Neuroexcitatory Amino Acid, in Toxic Mussels from Eastern Prince Edward Island’. Canadian Journal of Chemistry 67, no. 3 (1 March 1989): 481–90. https://doi.org/10.1139/v89-075.
- McCarron, Pearse, Stephen Burrell, and Philipp Hess. ‘Effect of Addition of Antibiotics and an Antioxidant on the Stability of Tissue Reference Materials for Domoic Acid, the Amnesic Shellfish Poison’. Analytical and Bioanalytical Chemistry 387, no. 7 (1 November 2006): 2495–2502. https://doi.org/10.1007/s00216-006-0833-3.
- Quilliam, Michael A., P. Greig Sim, Archibald W. McCulloch, and A. Gavin McInnes. ‘High-Performance Liquid Chromatography of Domoic Acid, a Marine Neurotoxin, with Application to Shellfish and Plankton’. International Journal of Environmental Analytical Chemistry 36, no. 3 (July 1989): 139–54. https://doi.org/10.1080/03067318908026867.
- Zaman, Lubna, Osamu Arakawa, Ako Shimosu, Yoshio Onoue, Sachio Nishio, Yasuo Shida, and Tamao Noguchi. ‘Two New Isomers of Domoic Acid from a Red Alga, Chondria Armata’. Toxicon 35, no. 2 (February 1997): 205–12. https://doi.org/10.1016/s0041-0101(96)00123-7.
- Thomas, Krista, Ruth Perez, Sheila Crain, Christopher Miles, and Pearse McCarron. ‘DA-h: Certified Calibration Solution for Domoic Acid’. National Research Council Canada, 29 July 2022. https://doi.org/10.4224/CRM.2022.DA-H.20210922.
- ‘Evaluation of Measurement Data — Guide to the Expression of Uncertainty in Measurement’, 2008. https://doi.org/10.59161/jcgm100-2008e.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 6594b278-6ed8-4547-9b4d-c8b98b1d0a9b |
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| Record created | 2026-01-26 |
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| Record modified | 2026-02-09 |
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