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DOLT-5: Dogfish Liver Certified Reference Material for Trace Metals and other Constituents

From National Research Council Canada

Alternative titleDOLT-5 : Foie de chien de mer, matériau de référence certifié pour les métaux traces et d'autres constituants
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DOIResolve DOI: https://doi.org/10.4224/crm.2014.dolt-5
AuthorSearch for: 1ORCID identifier: https://orcid.org/0000-0002-4351-2503; Search for: 1ORCID identifier: https://orcid.org/0000-0002-3376-0722; Search for: 1ORCID identifier: https://orcid.org/0000-0002-1167-6474; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-0083-0528; Search for: 1; Search for: 1; Search for: 1; Search for: 2; Search for: 3; Search for: 4; Search for: 4; Search for: 5, 6; Search for: 5; Search for: 7; Search for: 7; Search for: 8; Search for: 8; Search for: 8; Search for: 8; Search for: 1ORCID identifier: https://orcid.org/0000-0002-3349-5535; Search for: 1ORCID identifier: https://orcid.org/0000-0002-2377-2615
Affiliation
  1. National Research Council of Canada
  2. Forensic Chemistry Center, U.S. Food and Drug Administration, Cincinnati OH, USA
  3. Center for Food Safety and Applied Nutrition, U.S. Food and Drug Administration, College Park MD, USA
  4. University of Graz, Graz, Austria
  5. Matís, Research and Innovation, Reykjavik, Iceland
  6. University of Iceland, Reykjavik, Iceland
  7. Institute of Analytical Chemistry of the Czech Academy of Sciences, Brno, Czech Republic
  8. Brooks Applied Labs, Bothell WA, USA
Format3D, Material
SubjectCanadian reference material; DOLT-5; trace metals; dogfish liver; Squalus acanthias
Abstract
DOLT-5 is a dogfish (Squalus acanthias) liver Certified Reference Material (CRM) from the National Research Council of Canada with information on trace element and species content. A unit of DOLT-5 consists of approximately 20 grams of dogfish liver in an amber glass vial.
Analytes
View analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
aluminiummass fraction31.74.2mg/kgreference
antimonymass fraction0.013mg/kginformation
arsenicmass fraction34.62.4mg/kgcertified
arsenobetaine (as As)mass fraction24.20.8mg/kgcertified
inorganic arsenicmass fraction0.0340.002mg/kgcertified
dimethylarsinic acid (as As)mass fraction3.090.188mg/kgreference
monomethylarsonic acid (as As)mass fraction0.2010.024mg/kgreference
cadmiummass fraction14.50.6mg/kgcertified
calciummass fraction55080mg/kgcertified
chromiummass fraction2.350.58mg/kgreference
cobaltmass fraction0.2670.026mg/kgcertified
coppermass fraction35.02.4mg/kgcertified
ironmass fraction107080mg/kgcertified
leadmass fraction0.1620.032mg/kgcertified
magnesiummass fraction940100mg/kgcertified
manganesemass fraction8.910.70mg/kgreference
mercurymass fraction0.440.18mg/kgcertified
methylmercury (as Hg)mass fraction0.1190.058mg/kgreference
molybdenummass fraction1.410.22mg/kgcertified
nickelmass fraction1.710.56mg/kgreference
phosphorusmass fraction11500mg/kginformation
potassiummass fraction144003000mg/kgcertified
seleniummass fraction8.31.8mg/kgcertified
silvermass fraction2.050.08mg/kgcertified
sodiummass fraction99001600mg/kgcertified
strontiummass fraction3.730.26mg/kgcertified
thalliummass fraction0.013mg/kginformation
tinmass fraction0.0690.036mg/kgcertified
uraniummass fraction0.082mg/kginformation
vanadiummass fraction0.510.06mg/kgcertified
zincmass fraction105.35.4mg/kgcertified
Publication date
PublisherNational Research Council of Canada
Copyright statement
  • © 2014 National Research Council of Canada
Access condition
References
View items (3)
  1. Guide to the expression of uncertainty in measurement (GUM) (1 September 2008). .
  2. Gajdosechova, Zuzana, Patricia Grinberg, Kevin Kubachka, Mesay Wolle, Andrea Raab, Joerg Feldmann, Rebecca Sim, et al. ‘Determination of Inorganic As, DMA and MMA in Marine and Terrestrial Tissue Samples: A Consensus Extraction Approach’. Environmental Chemistry, 2023. .
  3. DerSimonian, Rebecca, and Nan Laird. ‘Meta-Analysis in Clinical Trials’. Controlled Clinical Trials 7, no. 3 (September 1986): 177–88. .
Referenced by
View items (3)
  1. Marschner, Karel, Ásta H. Pétursdóttir, Patrick Bücker, Andrea Raab, Jörg Feldmann, Zoltán Mester, Tomáš Matoušek, and Stanislav Musil. ‘Validation and Inter-Laboratory Study of Selective Hydride Generation for Fast Screening of Inorganic Arsenic in Seafood’. Analytica Chimica Acta 1049 (February 2019): 20–28. https://doi.org/10.1016/j.aca.2018.11.036.
  2. Kumkrong, Paramee, Benjaporn Thiensong, Phuong Mai Le, Garnet McRae, Anthony Windust, Suladda Deawtong, Juris Meija, Paulette Maxwell, Lu Yang, and Zoltán Mester. ‘Species Specific Isotope Dilution for the Accurate and SI Traceable Determination of Arsenobetaine and Methylmercury in Cuttlefish and Prawn’. Analytica Chimica Acta 943 (November 2016): 41–49. https://doi.org/10.1016/j.aca.2016.09.031.
  3. Gao, Ying, Ralph E. Sturgeon, Zoltán Mester, Enea Pagliano, Raphael Galea, Patrick Saull, Xiandeng Hou, and Lu Yang. ‘On-Line UV Photochemical Generation of Volatile Copper Species and Its Analytical Application’. Microchemical Journal 124 (January 2016): 344–49. https://doi.org/10.1016/j.microc.2015.09.020.
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CollectionCanadian Reference Materials and Methods
Record identifier78bfab6b-21cf-4733-a871-cac430f711f5
Record created2019-01-28
Record modified2024-04-04
Date modified: