| Alternative title | MESS-4 : Matériau de référence certifié pour la teneur en métaux totaux et extractibles des sédiments marins |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2014.mess-4 |
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| Author | Search for: Willie, Scott1ORCID identifier: https://orcid.org/0000-0002-3376-0722; Search for: Nadeau, Kenny1; Search for: Pihillagawa Gedara, Indumathi1; Search for: Yang, Lu1ORCID identifier: https://orcid.org/0000-0002-6896-8603; Search for: Clancy, Vincent1ORCID identifier: https://orcid.org/0000-0002-0083-0528; Search for: Grinberg, Patricia1ORCID identifier: https://orcid.org/0000-0002-1167-6474; Search for: Kumkrong, Paramee1; Search for: Mercier, Patrick H.J.1; Search for: Mihai, Ovidiu1; Search for: Tyo, Daniel D.1; Search for: Jiang, Cindy1; Search for: Kingston, David M.1; Search for: Meija, Juris1ORCID identifier: https://orcid.org/0000-0002-3349-5535; Search for: Maxwell, Paulette1; Search for: Mester, Zoltan1ORCID identifier: https://orcid.org/0000-0002-2377-2615 |
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| Affiliation | - National Research Council Canada
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| Format | 3D, Material |
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| Material type | Matrix material |
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| Subject | Canadian reference material; MESS-4; trace metals; marine sediment; butyltin |
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| Abstract | MESS-4 is a marine sediment Certified Reference Material (CRM) from the National Research Council Canada (NRC) with information on total and extractable metal content. A unit of MESS-4 consists of approximately 50 grams of marine sediment. |
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| Analytes | View analytes| Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| aluminium | mass fraction | 79100 | 2000 | mg/kg | certified | | antimony | mass fraction | 1.07 | 0.16 | mg/kg | certified | | arsenic | mass fraction | 21.7 | 2.8 | mg/kg | certified | | barium | mass fraction | 920 | | mg/kg | information | | beryllium | mass fraction | 2.09 | 0.28 | mg/kg | certified | | bismuth | mass fraction | 2.7 | | mg/kg | information | | bromine | mass fraction | 60 | | mg/kg | information | | caesium | mass fraction | 10 | | mg/kg | information | | cadmium | mass fraction | 0.28 | 0.04 | mg/kg | certified | | calcium | mass fraction | 13100 | 600 | mg/kg | certified | | carbon | mass fraction | 17900 | | mg/kg | information | | cerium | mass fraction | 72 | | mg/kg | information | | chlorine | mass fraction | 13100 | 4400 | mg/kg | certified | | chromium | mass fraction | 94.3 | 1.8 | mg/kg | certified | | cobalt | mass fraction | 13 | 0.8 | mg/kg | certified | | copper | mass fraction | 32.9 | 1.8 | mg/kg | certified | | dibutyltin (as Sn) | mass fraction | <0.005 | | mg/kg | information | | europium | mass fraction | 1.3 | | mg/kg | information | | gallium | mass fraction | 18 | | mg/kg | information | | germanium | mass fraction | 0.16 | | mg/kg | information | | hafnium | mass fraction | 3 | | mg/kg | information | | indium | mass fraction | 0.1 | | mg/kg | information | | iron | mass fraction | 37900 | 1600 | mg/kg | certified | | lanthanum | mass fraction | 35 | | mg/kg | information | | lead | mass fraction | 21.5 | 1.2 | mg/kg | certified | | lithium | mass fraction | 65.3 | 6.8 | mg/kg | certified | | lutetium | mass fraction | 0.11 | | mg/kg | information | | magnesium | mass fraction | 15800 | 1200 | mg/kg | certified | | manganese | mass fraction | 298 | 14 | mg/kg | certified | | mercury | mass fraction | 0.09 | 0.04 | mg/kg | reference | | molybdenum | mass fraction | 2.53 | 0.12 | mg/kg | reference | | monobutyltin (as Sn) | mass fraction | <0.05 | | mg/kg | information | | neodymium | mass fraction | 42 | | mg/kg | information | | nickel | mass fraction | 42.8 | 1.6 | mg/kg | certified | | niobium | mass fraction | 12 | | mg/kg | information | | phosphorus | mass fraction | 1040 | 160 | mg/kg | certified | | potassium | mass fraction | 23800 | 1000 | mg/kg | certified | | rhenium | mass fraction | 0.004 | | mg/kg | information | | rubidium | mass fraction | 180 | | mg/kg | information | | samarium | mass fraction | 5.5 | | mg/kg | information | | scandium | mass fraction | 13.4 | | mg/kg | information | | selenium | mass fraction | 1.5 | | mg/kg | information | | silicon | mass fraction | 278000 | 20 | mg/kg | certified | | silver | mass fraction | 0.161 | 0.024 | mg/kg | certified | | sodium | mass fraction | 12600 | 800 | mg/kg | certified | | strontium | mass fraction | 132 | 8 | mg/kg | certified | | sulfur | mass fraction | 1580 | 200 | mg/kg | certified | | tantalum | mass fraction | 1 | | mg/kg | information | | tellurium | mass fraction | 0.1 | | mg/kg | information | | thallium | mass fraction | 0.85 | 0.1 | mg/kg | certified | | thorium | mass fraction | 12 | | mg/kg | information | | tin | mass fraction | 2.35 | 0.12 | mg/kg | certified | | titanium | mass fraction | 3840 | 220 | mg/kg | certified | | tributyltin (as Sn) | mass fraction | <0.005 | | mg/kg | information | | tungsten | mass fraction | 1.3 | | mg/kg | information | | uranium | mass fraction | 3.4 | 0.4 | mg/kg | certified | | vanadium | mass fraction | 216 | 8 | mg/kg | certified | | ytterbium | mass fraction | 2 | | mg/kg | information | | yttrium | mass fraction | 20 | | mg/kg | information | | zinc | mass fraction | 147 | 6 | mg/kg | certified | | zirconium | mass fraction | 96 | | mg/kg | information |
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| Publication date | 2014-11-01 |
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| Publisher | National Research Council Canada |
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| Copyright statement | - © 2014
National Research Council Canada
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| Access condition | |
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| References | View items (6)- 1. Evaluation of measurement data: Guide to the expression of uncertainty in measurement JCGM100:2008 (1 September 2008). https://www.bipm.org/en/publications/guides/gum.html.
- Kumkrong, Paramee, Patrick H.J. Mercier, Indu Pihilligawa Gedara, Ovi Mihai, Daniel D. Tyo, Jiang Cindy, David M. Kingston, and Zoltán Mester. ‘Determination of 27 Metals in HISS-1, MESS-4 and PACS-3 Marine Sediment Certified Reference Materials by the BCR Sequential Extraction’. Talanta 221 (January 2021): 121543. https://doi.org/10.1016/j.talanta.2020.121543.
- Kumkrong, Paramee, Ovi Mihai, Patrick H. J. Mercier, Indu Gedara Pihilligawa, Daniel D. Tyo, and Zoltán Mester. ‘Tessier Sequential Extraction on 17 Elements from Three Marine Sediment Certified Reference Materials (HISS-1, MESS-4, and PACS-3)’. Analytical and Bioanalytical Chemistry 413, no. 4 (24 November 2020): 1047–57. https://doi.org/10.1007/s00216-020-03063-z.
- DerSimonian, Rebecca, and Nan Laird. ‘Meta-Analysis in Clinical Trials’. Controlled Clinical Trials 7, no. 3 (September 1986): 177–88. https://doi.org/10.1016/0197-2456(86)90046-2.
- Possolo, Antonio, and Blaza Toman. ‘Assessment of Measurement Uncertainty via Observation Equations’. Metrologia 44, no. 6 (7 November 2007): 464–75. https://doi.org/10.1088/0026-1394/44/6/005.
- Thompson, Michael, and Stephen L. R. Ellison. ‘Dark Uncertainty’. Accreditation and Quality Assurance 16, no. 10 (12 July 2011): 483–87. https://doi.org/10.1007/s00769-011-0803-0.
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| Referenced by | View items (1)- Gao, Ying, Mo Xu, Ralph E. Sturgeon, Zoltán Mester, Zeming Shi, Raphael Galea, Patrick Saull, and Lu Yang. ‘Metal Ion-Assisted Photochemical Vapor Generation for the Determination of Lead in Environmental Samples by Multicollector-ICPMS’. Analytical Chemistry 87, no. 8 (31 March 2015): 4495–4502. https://doi.org/10.1021/acs.analchem.5b00533.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 8a3fd39a-c068-4ce0-820c-d08cf742a20a |
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| Record created | 2019-01-28 |
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| Record modified | 2025-11-20 |
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