| Alternative title | DONN-1 : Matériau de référence certifié – solution d’étalonnage de 4-désoxynivalénol |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2022.donn-1 |
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| Author | Search for: Bahadoor, Adilah1ORCID identifier: https://orcid.org/0000-0002-8130-5070; Search for: Rajotte, Isabelle1; Search for: Bates, Jennifer1; Search for: Watt, Sarah1; Search for: Meija, Juris1ORCID identifier: https://orcid.org/0000-0002-3349-5535; Search for: Melanson, Jeremy1ORCID identifier: https://orcid.org/0000-0002-2290-0101 |
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| Affiliation | - National Research Council of Canada
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| Format | 3D, Material |
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| Subject | Canadian reference material; DONN-1; 4-deoxynivalenol |
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| Abstract | DONN-1 is a calibration solution certified reference material (CRM) for the regulated mycotoxin 4 deoxynivalenol, in acetonitrile. The calibration solution is intended for method development and instrument calibration to produce accurate and traceable measurements for 4-deoxynivalenol. Certified values for the mass fraction and mass concentration of 4-deoxynivalenol in DONN-1 have been established. |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| 4-deoxynivalenol | mass fraction | 54.4 | 2.6 | µg/g | certified | | 4-deoxynivalenol | mass concentration | 42.0 | 2.2 | µg/mL | certified |
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| Publication date | 2022-07-01 |
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| Publisher | National Research Council of Canada |
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| Copyright statement | - © 2022
National Research Council of Canada
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| Access condition | |
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| References | View items (4)- Bahadoor, Adilah, Sarah Watt, Isabelle Rajotte, and Jennifer Bates. ‘Tautomerization and Isomerization in Quantitative NMR: A Case Study with 4-Deoxynivalenol (DON)’. Journal of Agricultural and Food Chemistry 70, no. 8 (16 February 2022): 2733–40. https://doi.org/10.1021/acs.jafc.1c08053.
- Bahadoor, Adilah, Andreas Brinkmann, and Jeremy E. Melanson. ‘13C-Satellite Decoupling Strategies for Improving Accuracy in Quantitative Nuclear Magnetic Resonance’. Analytical Chemistry 93, no. 2 (10 December 2020): 851–58. https://doi.org/10.1021/acs.analchem.0c03428.
- Guide to the expression of uncertainty in measurement (GUM) (1 September 2008). https://www.bipm.org/en/publications/guides.
- Veen, Adriaan M. H. van der. ‘Bayesian Analysis of Homogeneity Studies in the Production of Reference Materials’. Accreditation and Quality Assurance 22, no. 6 (2 November 2017): 307–19. https://doi.org/10.1007/s00769-017-1292-6.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 9db679b9-4412-45fa-89a4-4a4dc361936a |
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| Record created | 2022-07-25 |
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| Record modified | 2024-07-17 |
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