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DA-h: Certified Calibration Solution for Domoic Acid

From National Research Council Canada

Alternative titleDA-h : Solution d’étalonnage certifiée pour l’acide domoïque
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DOIResolve DOI: https://doi.org/10.4224/crm.2022.da-h.20210922
AuthorSearch for: 1ORCID identifier: https://orcid.org/0000-0002-4850-5863; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: 1ORCID identifier: https://orcid.org/0000-0001-8537-4439; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council of Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; CRM-DA-h; amnesic shellfish poisoning; domoic acid
Abstract
CRM-DA-h is a certified calibration solution designed for analytical method development and accurate quantitation of DA. The concentration is suitable for preparing a dilution series for calibration of instruments such as liquid chromatography with detection by ultraviolet absorbance (LC–UV) or mass spectrometry (LC–MS), as well as for spiking control samples for recovery experiments.
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
domoic acid and C5'-epi-domoic acidmass fraction97.95.5µg/gcertified
domoic acid and C5'-epi-domoic acidmass concentration (15-30 °C)97.15.5µg/mLcertified
domoic acid and C5'-epi-domoic acidconcentration (15-30 °C)31218µmol/Lcertified
domoic acid (DA)mass concentration (15-30 °C)96.6µg/mLinformation
C5'-epi-domoic acidmass concentration (15-30 °C)0.55µg/mLinformation
isodomoic acid Emass concentration (15-30 °C)0.19µg/mLinformation
isodomoic acid Dmass concentration (15-30 °C)0.82µg/mLinformation
isodomoic acid Amass concentration (15-30 °C)1.1µg/mLinformation
Publication date
PublisherNational Research Council of Canada
Copyright statement
  • © 2022 National Research Council of Canada
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References
View items (8)
  1. Quilliam, Michael A., and Jeffrey L. C. Wright. ‘The Amnesic Shellfish Poisoning Mystery’. Analytical Chemistry 61, no. 18 (15 September 1989): 1053A-1060A. .
  2. Wright, J. L. C., R. K. Boyd, A. S. W. de Freitas, M. Falk, R. A. Foxall, W. D. Jamieson, M. V. Laycock, et al. ‘Identification of Domoic Acid, a Neuroexcitatory Amino Acid, in Toxic Mussels from Eastern Prince Edward Island’. Canadian Journal of Chemistry 67, no. 3 (1 March 1989): 481–90. .
  3. Quilliam, Michael A., Bruce A. Thomson, George J. Scott, and K. W. Michael Siu. ‘Ion‐spray Mass Spectrometry of Marine Neurotoxins’. Rapid Communications in Mass Spectrometry 3, no. 5 (May 1989): 145–50. .
  4. Quilliam, Michael A., P. Greig Sim, Archibald W. McCulloch, and A. Gavin McInnes. ‘High-Performance Liquid Chromatography of Domoic Acid, a Marine Neurotoxin, with Application to Shellfish and Plankton’. International Journal of Environmental Analytical Chemistry 36, no. 3 (July 1989): 139–54. .
  5. Quilliam, Michael A, Mie Xie, and William R Hardstaff. ‘Rapid Extraction and Cleanup for Liquid Chromatographic Determination of Domoic Acid in Unsalted Seafood’. Journal of AOAC INTERNATIONAL 78, no. 2 (1 March 1995): 543–54. .
  6. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  7. Falk, Michael, John A. Walter, and Paul W. Wiseman. ‘Ultraviolet Spectrum of Domoic Acid’. Canadian Journal of Chemistry 67, no. 9 (1 September 1989): 1421–25. .
  8. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
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CollectionCanadian Reference Materials and Methods
Record identifiera378a45e-91d2-46f0-be8e-15bef03f3216
Record created2022-07-29
Record modified2025-04-16
Date modified: