| Alternative title | YTX-d : Solution d’étalonnage certifiée pour la yessotoxine |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2024.ytx-d.20231207 |
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| Author | Search for: Giddings, Sabrina D1; Search for: Crain, Sheila1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: McCarron, Pearse1ORCID identifier: https://orcid.org/0000-0002-7746-8432 |
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| Affiliation | - National Research Council Canada
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| Format | 3D, Material |
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| Subject | Canadian reference material; yessotoxin; YTX; YTX-d |
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| Abstract | CRM-YTX-d is a certified calibration solution for analytical method development and accurate quantitation of YTX. The concentration is suitable for preparing a dilution series for calibration of instruments such as liquid chromatography–mass spectrometry (LC–MS), and for spiking control samples for recovery experiments. |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| yessotoxin | mass fraction | 6.01 | 0.32 | µg/g | certified | | yessotoxin | mass concentration (15-30 °C) | 4.74 | 0.26 | µg/mL | certified | | yessotoxin | concentration (15-30 °C) | 4.15 | 0.23 | µmol/L | certified |
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| Publication date | 2024-06-12 |
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| Publisher | National Research Council of Canada |
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| Copyright statement | - © 2024 National Research Council of Canada
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| Access condition | |
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| References | View items (7)- Hess, Philipp, and John A. B. Aasen. ‘Chemistry, Origins, and Distribution of Yessotoxin and Its Analogues’. Phycotoxins: Chemistry and Biochemistry, 24 March 2007, 187–202. https://doi.org/10.1002/9780470277874.ch10.
- Regulation (EC) No 853/2004 of the European parliament and of the council of 29 April 2004 laying down specific hygiene rules for food of animal origin (30 April 2004). https://eur-lex.europa.eu/eli/reg/2004/853/oj.
- Commission Regulation (EU) No 786/2013 of 16 August 2013 amending Annex III to Regulation (EC) No 853/2004 of the European Parliament and of the Council as regards the permitted limits of yessotoxins in live bivalve molluscs (16 August 2013). https://data.europa.eu/eli/reg/2013/786/oj.
- Miles, Christopher O., Alistair L. Wilkins, Dwayne J. Jensen, Janine M. Cooney, Michael A. Quilliam, John Aasen, and A. Lincoln MacKenzie. ‘Isolation of 41a-Homoyessotoxin and the Identification of 9-Methyl-41a-Homoyessotoxin and Nor-Ring A-Yessotoxin from Protoceratium Reticulatum’. Chemical Research in Toxicology 17, no. 11 (15 October 2004): 1414–22. https://doi.org/10.1021/tx049832r.
- Giddings, Sabrina, Sheila Crain, and Pearse McCarron. ‘YTX-c: Certified Calibration Solution for Yessotoxin’. National Research Council of Canada, 12 February 2016. https://doi.org/10.4224/CRM.2016.YTX-C.20151125.
- Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. https://doi.org/10.1021/ac048385h.
- Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. https://doi.org/10.1007/s007690050020.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | ea19c185-12ee-4792-9139-7ca6310ad0e0 |
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| Record created | 2024-06-25 |
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| Record modified | 2024-07-10 |
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