| Alternative title | 15DON-1 : Matériau de référence certifié d’une solution d’étalonnage pour le 15-acétyl-4-déoxynivalénol |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2025.15don-1 |
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| Author | Search for: Bahadoor, Adilah1ORCID identifier: https://orcid.org/0000-0002-8130-5070; Search for: Bates, Jennifer1ORCID identifier: https://orcid.org/0000-0001-7650-2232 |
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| Affiliation | - National Research Council of Canada
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| Format | 3D, Material |
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| Material type | Calibration solution |
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| Subject | Canadian reference material; 15DON-1; 15-acetyl-4-deoxynivalenol; mycotoxins; food safety |
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| Abstract | 15DON-1 is a calibration solution certified reference material (CRM) for the mycotoxin 15-acetyl-4-deoxynivalenol, in acetonitrile. This mycotoxin is produced by the widespread fungal crop pathogen Fusarium graminearum and is monitored in the food supply. The material, distributed in 1 mL units, is intended for method development and instrument calibration to produce accurate and traceable measurements for 15-acetyl-4-deoxynivalenol. Certified values for the mass fraction and mass concentration of 15-acetyl-4-deoxynivalenol in 15DON-1 have been established. |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| 15-acetyl-4-deoxynivalenol | mass fraction | 115.2 | 4.3 | µg/g | certified | | 15-acetyl-4-deoxynivalenol | mass concentration (20 °C) | 90.0 | 3.7 | µg/mL | certified |
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| Period of validity | - Valid from 2025-10-10 until 2029-07-31
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| Storage conditions | |
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| Publication date | 2025-10-10 |
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| Publisher | National Research Council of Canada |
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| Copyright statement | - © 2025
National Research Council of Canada
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| Access condition | |
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| References | View items (3)- Bahadoor, Adilah, Sarah Watt, Isabelle Rajotte, and Jennifer Bates. ‘Tautomerization and Isomerization in Quantitative NMR: A Case Study with 4-Deoxynivalenol (DON)’. Journal of Agricultural and Food Chemistry 70, no. 8 (16 February 2022): 2733–40. https://doi.org/10.1021/acs.jafc.1c08053.
- DerSimonian, Rebecca, and Nan Laird. ‘Meta-Analysis in Clinical Trials’. Controlled Clinical Trials 7, no. 3 (September 1986): 177–88. https://doi.org/10.1016/0197-2456(86)90046-2.
- ‘Evaluation of Measurement Data — Guide to the Expression of Uncertainty in Measurement’, 2008. https://doi.org/10.59161/jcgm100-2008e.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | eed791ce-1052-4e1d-b187-88fdd540d702 |
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| Record created | 2025-10-14 |
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| Record modified | 2025-10-15 |
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